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    nbsp 0183 32 The skeleton carbonate was reduced to a fine powder using a Planetary Micro Mill PULVERISETTE 7 with metal cups filled with 0 5 cm balls that upon rotation milled down the samples...

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    nbsp 0183 32 blended in a HAAKE Rheomix internal mixer operating at a rotor speed of 60 rpm and 170 C during 5 min Obtained compounds were cooled to room temperature and then ground in a knife mill SM 300 Retch Germany at a speed of 2200 rpm...

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